MS 2041 Introduction to Crystal Structure and Diffraction Theories

Objective

The purpose of this course is to provide students fundamental knowledge of essential crystallography and X-ray diffraction theory.?The experimental techniques of X-ray diffraction and their applications in determination of crystal structure, lattice parameters, chemical compositions and residual stress will also be covered.

Textbook

B.D. Cullity and S.R. Stock," Elements of X-ray Diffraction", 3rd edition, Prentice Hall, 2001.

Reference Books

D. Mckie and C. Mckie, "Essentials of Crystallography", Blackwell Scientific Publications, 1986

M. M. Woolfson, “An Introduction to X-Ray Crystallography”, Cambridge University Press, 1970

余樹楨,"晶體之結構與性質",渤海堂文化公司,1989

Outline

Introduction:

Crystallography and x-ray technique

Essential Crystallography:

(1) Crystal lattices; (2) Crystal symmetry; (3) Stereographic projection

X-ray Diffraction Theory:

(1) Scattering of X-rays; (2) Bragg’s law; (3) Reciprocal space and reciprocal lattices; (4) Diffraction from a crystal – structure-factor calculations; (5) Factors affecting X-ray intensities

X-ray Experimental Methods:

(1) Diffractometer measurement; (2) Powder photographs; (3) Laue photographs

X-ray Diffraction Applications

(1) Determination of crystal structure; (2) Measurement of lattice parameters; (3) Chemical analysis; (4) Crystal size analysis; (5) Measurement of residual stress

Class notes

Lecture 1

Lecture 2

Lecture 3

Lecture 4

Lecture 5

Lecture 6

Lecture 7

Lecture 8

 

 

 

 

Previous exams

96 Midterm 1

96 Midterm 2

96 Final

Quiz

97 Midterm 1

97 Midterm 2

97 Final